Part 1 Introduction 1.1 General Rules for the Organic Chemistry Lab 1.2 General Lab Safety 1.3 Disposal of Lab Waste 1.4 Common Lab Equipment and Apparatus 1.5 Drying and Drying Agents 1.6 Heating and Cooling 1.7 Experimental Record and Laboratory Report 1.8 Chemical Literature Part 2 Basic Experimental Techniques 2.1 Melting Point 2.2 Recrystallization 2.3 Simple Distillation and Fractional Distillation 2.4 Steam Distillation 2.5 Vacuum Distillation 2.6 Solvent Extraction and Solution Washing 2.7 Sublimation 2.8 Refractive Index of Liquids 2.9 Chromatographic Techniques 2.10 Spectroscopic Identification of Organic Compound Part 3 Experiments 3.1 Synthesis of Cyclohexene 3.2 Synthesis of n-Butyl Bromide 3.3 Synthesis of Triphenylmethanol 3.4 Synthesis of Dibutyl Ether 3.5 Synthesis of Benzoic Acid and Benzyl Alcohol 3.6 Synthesis of Acetophenone 3.7 Synthesis of Adfpic Acid 3.8 Synthesis of Cinnamic Acid 3.9 Synthesis of Acetylsalicylic Acid (Aspirin) 3.10 Synthesis of Ethyl Acetate 3.11 Synthesis of n-Butyl Acetate 3.12 Synthesis of Ethyl Acetoacetate 3.13 Synthesis of Acetanilide 3.14 Synthesis of p-Acetylaminobenzenesulfonyl Chloride 3.15 Synthesis of p-Aminobenzenesulfonamide (Sulfanilamide) 3.16 Isolation of Caffeine From Tea Leaves 3.17 Synthesis of 2-Furanmethanol and 2-Furoic Acid 3.18 Synthesis of Methyl Orange Part 4 Appendix 4.1 Experiments from the Literature 4.1.1 A Microscale Synthesis of the Diastereomers of 2, 3-Dibromosuccinic Acid 4.1.2 A Multistep Synthesis of 4-Nitro-1-ethynylbenzene Involving Palladium Catalysis Conformational Analysis, Acetal Hydrolysis, and Oxidative Decarbonylation 4.1.3 A Safe Simple Halogenation Experiment 4.1.4 A Grignard-like Organic Reaction in Water 4.1.5 An Efficient Microscale Procedure for the Synthesis of Aspirin 4.1.6 A Solvent-Free Claisen Condensation Reaction 4.1.7 Convenient Synthesis of a Lactone, y-Butyrolactone 4.1.8 The Preparation of a Fluorescent Dye: A Microscale TLC Experiment 4.1.9 Polyester (PET) Synthesis 4.1.10 Microwave Microscale Experiment--2-Naphthy1 Acetate from 2-Naphthol 4.1.11 Fries Rearrangement AcCelerated by Microwave Radiation 4.2 List of The Elements with Their Symbols and Atomic Masses 4.3 Main Families of Organic Compounds 目录 第一部分 有机化学实验的一般知识 1·1 有机化学实验的基本规则 1·2 有机化学实验的一般安全知识 1·3 有机化学实验废物的处置 1·4 常用的玻璃仪器和实验装置 1·5 干燥与干燥剂 1·6 加热与冷却 1·7 实验记录和实验报告 1·8 有机化学的文献资料 第二部分 基本操作 2·1 熔点的测定 2·2 重结晶和过滤 2·3 蒸馏与分馏 2·4 水蒸气蒸馏 2·5 减压蒸馏 2·6 萃取与洗涤 2·7 升华 2·8 液体化合物折光率的测定 2·9 色谱技术 2·10 有机化合物的光谱鉴定 第三部分 有机化合物的制备 3·1 环己烯的制备 3·2 1-溴丁烷的制备 3·3 三苯甲醇的制备 3·4 正丁醚的制备 3·5 苯甲醇和苯甲酸的制备 3·6 苯乙酮的制备 3·7 己二酸的制备 3·8 肉桂酸的制备 3·9 乙酰水杨酸(阿司匹林)的制备 3·10 乙酸乙酯的制备 3·11 乙酸正丁酯的制备 3·12 乙酰乙酸乙酯的制备 3·13 乙酰苯胺的制备 3·14 对乙酰氨基苯磺酰氯的制备 3·15 对氨基苯磺酰胺(磺胺)的制备 3·16 从茶叶中提取咖啡因 3·17 呋喃甲醇和呋喃甲酸的制备 3·18 甲基橙的制备 第四部分 附录 4·1 有机化学实验操作(上)考试复习题 4·2 有机化学实验操作(下)考试复习题
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