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Physical Chemistry Combined Experiments(物理化学组合实验)
  • 书号:9787030678256
    作者:王舜
  • 外文书名:
  • 丛书名:
  • 装帧:平装
    开本:16
  • 页数:242
    字数:403000
    语种:en
  • 出版社:科学出版社
    出版时间:2021-08-01
  • 所属分类:
  • 定价: ¥89.00元
    售价: ¥89.00元
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本书对实验内容采用组合式编排,即以一种或一类物质的多种物性或一种物性的多种测量方法构成系列实验,同时对每个实验提供扩展性实验设计策略。根据教学需要可对基础、设计、综合三个层次的实验灵活选择组合,以培养学生综合分析问题和解决问题的能力。
  全书分为绪论、组合实验系列和附录。组合实验系列包括7个系列共34个实验。附录包括6个物理化学实验技术专题和24个常用的重要物理化学数据表。
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目录

  • Contents
    Preface
    Introduction 1
    Section 1 Purpose, requirements and rules of physical chemistry experiments 1
    Section 2 Safety protection of physical chemistry experiments 4
    Section 3 Errors and data processing in physical chemistry experiments 9
    Section 4 Computer processing of physical chemistry experiment data 20
    Combined experiment Ⅰ 23
    Experiment 1 Determination of the heat of combustion of sucrose by constant volume thermal method 23
    Experiment 2 Determination of the molar mass of sucrose by freezing point depression method 29
    Experiment 3 Determination of the rate constant of the acid-catalyzed conversion reaction of sucrose by optical rotation method 33
    Experiment 4 Determination of the Michaelis constant of sucrase by spectrophotometry 38
    Combined experiment Ⅱ 43
    Experiment 5 Determination of saturated vapor pressure of ethyl acetate by static method 43
    Experiment 6 Evaporation and condensation method to draw the equilibrium phase diagram of ethyl acetate-ethanol two-liquid system 46
    Experiment 7 Determination of the rate constant and activation energy of ethyl saponification by conductivity method 51
    Experiment 8 Determination of the dipole moment of ethyl acetate by the solution method 55
    Combined experiment Ⅲ 64
    Experiment 9 Determination of standard entropy and sublimation enthalpy of crystal iodine 64
    Experiment 10 Determination of I2 distribution coefficient anddissociation constant 68
    Experiment 11 Determination of the order of acetone iodization reactions 71
    Experiment 12 “Iodine Clock” reaction 76
    Combined experiment Ⅳ 81
    Experiment 13 Determination of partial molar volume of NaCl 81
    Experiment 14 Determination of osmotic pressure of NaCl injection 85
    Experiment 15 Phase analysis of X-ray powder diffraction method of NaCl 89
    Experiment 16 Drawing of three-component equilibrium phase diagram of KCl-HCl-H2O 95
    Experiment 17 Determination of the heat of solution for KNO3 99
    Combined experiment Ⅴ 104
    Experiment 18 Production and application of thermocouple 104
    Experiment 19 Drawing of two-component metal phase diagram 108
    Experiment 20 Determination of the electromotive potential of the original battery 111
    Experiment 21 Surface modification and coloration of aluminum anodization 116
    Experiment 22 Pyrophosphate copper plating 121
    Experiment 23 Stainless steel electrolytic polishing and waste liquid treatment 124
    Experiment 24 Synthesis, characterization and electrical properties of silver nano cables 129
    Combined experiment Ⅵ 134
    Experiment 25 Determination of surface tension of solution 134
    Experiment 26 Determination of critical micelle concentration of surfactants 140
    Experiment 27 Preparation and stability of sol 143
    Experiment 28 Determination of sol electric potential 149
    Experiment 29 Preparation and properties of emulsion 153
    Experiment 30 Determination of the average molar mass of polymer compounds 156
    Combined experiment Ⅶ 163
    Experiment 31 Determination of magnetic susceptibility 163
    Experiment 32 Biomineral and biomineralization 168
    Experiment 33 Synthesis and structure analysis of KDP crystals 172
    Experiment 34 Molecular model and crystal structure 176
    References 181
    Appendix 1 Special topic of physical chemistry experiment technology 183
    Special Topic Ⅰ Temperature measurement technology and instruments 183
    Special Topic Ⅱ Pressure measurement technology and instruments 189
    Special Topic Ⅲ Density measurement technology and instruments 201
    Special Topic Ⅳ Electrical measurement technology and instruments 204
    Special Topic Ⅴ Optical measurement technology and instruments 217
    Special Topic Ⅵ Viscosity measurement technology and instruments 227
    Appendix 2 Data sheets commonly used in physical chemistry experiments 233
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